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Lignocellulosic compound dissolution produces a reduction/disappearance of some vibrational bands. Obtained results suggest that acid hydrolysis breaks down the lignocellulosic compounds from the coffee parchment, and alkaline hydrolysis allows the solubilization of lignin and hemicellulose. TGA, SEM, XRD, and FT-IR techniques allowed for characterizing the coffee parchment hydrolyzed and bleached. Factorial design experiments allowed studying the influence of the chemical precursor concentrations and reaction times on the mass losses. Cellulose microfibrils were isolated from coffee parchment through acid hydrolysis, alkaline hydrolysis, and bleaching. |
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